Anhui Rencheng Technology Co., Ltd.

Urumogi rutera CAS: 28578-16-7 Ethyl Glycidate Amavuta ya Pmk

Ibisobanuro bigufi:

Unyandikire: Anhui Rencheng Technology Co., Ltd.
WhatsApp / Wechat / Telegaramu: +8615656977652
Wickr Me: weichengju
Email:002@ahrencheng.com

Izina ryibicuruzwa: PMK ethyl glycidate
CAS: 28578-16-7
Inzira ya molekulari: C13H14O5
Uburemere bwa molekuline: 227.1


Ibicuruzwa birambuye

Ibicuruzwa

Amakuru Yibanze

izina RY'IGICURUZWA

2-Bromo-4'-methylpropiophenone

URUBANZA

1451-82-7

EINECS

696-162-0

Inzira ya molekulari

C10H11BrO

Uburemere bwa molekile

227.1

Ingingo yo guteka

75-77ºC

Ingingo ya Flash

59 ° C.

Kugaragara

Ifu ya kirisiti yera

PSA

17.07000

LogP

3.00

Imiterere yo kubika

Firigo

Ibikoresho

Imiti yinganda / Imikorere ihuza ibikorwa

Imikorere

Ahanini ukoreshe muri Pharmaceutical Intermediates / ubuvuzi hagati

1) Kurinda argon, ongeramo (4g, 30mmol) ya anhidrous aluminium chloride kuri flask ya reaction, hanyuma ushyiremo 20ml ya dichloromethane ya anhydrous, hanyuma ukangure gushonga.Nyuma yo gushonga, ongeramo (1.7g, 10mmol) 2-bromopropionyl chloride, hanyuma ukomeze kubyutsa iminota 20.Hanyuma (0,92g, 10mmol) toluene yongeweho, hanyuma iyongerwaho ryarangiye bitonyanga muminota 30.Nyuma yo kugabanuka gutonyanga birangiye, kugaruka kuri 2H, no gukonjesha ubushyuhe bwicyumba nyuma yo kugaruka kurangiye.

2) Nyuma yo gukonjesha, suka igisubizo muri 40ml y'amazi ya barafu, ongeramo 20ml ya dichloromethane na 20ml ya acide hydrochloric 6N, uzunguze cyane hanyuma uhagarare hanyuma utandukane mubice.Nyuma yo gutondeka, icyiciro cya dichloromethane cyurwego rwo hasi hasigaye.Nyuma yo koza icyiciro cya dichloromethane hamwe na 1NHCL inshuro ebyiri, yumishijwe na sulfate ya anhidrous magnesium sulfate, kuyungurura, no kuzunguruka kugirango ibone ibintu byamavuta bibonerana.

3) Shira ibintu bibonerana mumasahani ya kristu hanyuma wongereho ether kugirango ushonga, hanyuma wongereho buhoro buhoro ether ya peteroli kugeza ubaye muke, gutwikira no gukata urupapuro kugirango uhagarare mumyuka ya fume kugirango uhindurwe kugirango ubone 1.37g yibicuruzwa 2-bromo -4 '-Ibikoresho bisobanutse bya methyl phenylacetone.

Imiti-yimiti-CAS-1451-82-7-mububiko-hamwe-hejuru-Ubwiza- (4)

Porogaramu

2-Bromo-4'-methylpropiophenone irashobora gukoreshwa nkigihe gito muguhuza imiti.Nko gutegura methylmethcathinone (4-MMC), izwi kandi nka Mephedrone (Mephedrone), andi mazina arimo 2-Bromo-1- (p-tolyl) propan-1-imwe, 2-Bromo-4'-methylpropiophenone , EY1 & VR D1 cyangwa CAS 1451-82-7.

Gupakira & Kohereza

gupakira

Ibibazo

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